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Keywords

Oxidation, Toughness, Ferroelasticity

出版物2004年以降のNIMS所属における研究成果や出版物を表示しています。

口頭発表

    所属学会

    日本航空宇宙学会, Minerals,Metals & Materials Society

    構造材料研究センター
    タイトル

    Assessment of Cracking in Additively Manufactured Metals and Alloys

    キーワード

    Additive Manufacturing, Inconel 738LC, Tungsten, Cracking

    概要

    ● Evaluation of process parameters to mitigate cracking in metals and alloys fabricate via laser powder bed fusion (L-PBF).

    ● Analysis of microstructure, cracking, chemical segregation in metallic materials fabricated via L-PBF via scanning and transmission electron microscopy and atom probe tomography.

    新規性・独創性

    ● Fabrication of metals such as nickel-based superalloys and tungsten via laser printing is challenging due to the prevalence of cracking in these materials.

    ● Cracking can be caused by the very high cooling rates and thermal gradients of the AM process, repeated melting/re-melting, and chemical segregation during solidification.

    内容

    image

    Ductility-dip cracking (DDC) is a type of solid-state cracking with corresponding ductility loss that is associated with solidification processes in FCC metals and alloys. The phenomenon typically occurs at 0.5 – 0.7 of the alloy melting point. The prevalence of this type of cracking during the tensile deformation of additively manufactured Inconel 738LC at elevated temperature has been studied. Transmission electron microscopy analysis of Inconel 738LC fabricated by L-PBF revealed the presence Ni, Al and Ti (gamma prime-forming elements) along the high-angle grain boundaries following tensile testing at 900ºC. It is therefore surmised that a thin layer of gamma-prime formed along the grain boundaries in the additively manufactured material and weakened the boundaries, thereby facilitating intergranular ductility-dip cracking.

    Samples of pure tungsten with the constricted specimen geometry shown in the figure were fabricated by L-PBF using a substrate pre-heating temperature of 530ºC and scan rotation angles of 90º and 67º. Results indicate that a combination of both substrate pre-heating and a constricted geometry may lead to reduced cracking in samples fabricated using a rotation angle of 67º. The effects of these parameters on material fabricated using a scan rotation angle of 90º, however, appear to be negligible.

    image

    まとめ

    ● Microstructural analysis of additively manufactured metals and alloys can determine cracking mechanisms and causes such as rapid solidification, phase precipitation or elemental segregation.

    ● A detailed understanding of these cracking mechanisms in turn enables optimization of process parameters to mitigate and ultimately eliminate cracking in additively manufactured metallic materials.

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    この機能は所内限定です。

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